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1 Mon Ju1
1 Mon Jul 18 910
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1 Mon Jul 18 1233
1 Mon Jul 18 794
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1 Mon Jul 18 1175
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1 Mon Jul 18 1120
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1 Fri Jul 15 929
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1 Fri Jul 15 1038
1 Fri Jul 15 1213
1 Fri Jul 15 1420
1 Fri Jul 15 1189
1 Fri Jul 15 834
1 Fri Jul 15 1146
1 Fri Jul 15 1064
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1 Wed Jul 13 851
1 Wed Jul 13 1223
our compound is high 69Thu Jul 28
If our compound contains some impurities , then how can we come to isolate the pure one from TLC 3Tue Feb 19
How can l remove salts (Li) from free amino acid? 1Sat Jun 9
when I did 19F NMR I saw broad peak. What are the cuase to form that 4Thu Oct 16
Is N-phenylglycine and L-(alpha) phenylglycine are same? 2Thu Jun 7
What is meant by Nitrogen atmosphere, means if we carry out the reaction in Nitrogen atmosphere, how can we go through? 1Mon Jul 16
How do synthesize N-Phenylglycine from anilne and chlroacetic acid OR aniline and ethyl chloroacetate 0Thu May 31
If we not get the spot for reactant , then what its mean? 4Fri Dec 26
why all naturally occuring sugars are d-form? 1Fri Sep 14
Best way to get rid of TMSCN from a reaction when used in excess? 1Mon Jul 21
What is the procedure to quench raney nickel (deactivate completely)after reaction in large scale. 3Fri Dec 26
What is the mildest workup method to remove formic acid from a reaction mixture containing palladium carbon and methanol? 1Fri May 4
Why do the spots / compounds seperate in ethyl ether 0Fri Apr 6
why do i get so much dimerization of alkyne in Sonogashira? I degas my solvents and use high-purity reagents 3Wed Nov 19
What is the best method for removal of the hydrazinedicarboxylate byproduct following Mitsunobu? Even if the Rf of my product is much higher, I still have contamination after column chromatography. 1Wed Aug 15
Does anyone have a good method for removing silanol byproducts other than chromatography? 3Tue Feb 19
My product is in almost neutral solution or may be silghtly basic PH 8-9 can I use ethyl acetate as extracting solvent my compound is soluble in ethyl acetate and in water 3Tue Feb 19
what is polar 2Sun Jan 27
My compund shows thick line in the TLC and I do not see any separated spot. I have also tried with all possible solvents and still i face the problem but am sure that my comund has impurity which can not be separated in TLC. what to do? 4Thu Jun 7
My column takes to much solvent & fraction are very very dilute what can i do. 3Wed Mar 28
my aqueos extract spots never seem to migrate with any solvent system, even if they do, it is to a very less extent. What should i do? 1Mon Feb 26
how we could tell by looking at tlc that our reaction is complete? 2Mon Jun 4
which elluent can be used for to separate phenol , hydroquinone, catechol and quinone 0Tue Nov 28
my compound have two chloro groups react with amine which chloro group is protected 0Mon Nov 27
my reaction given nonpolar spots how to remove 0Mon Nov 27
my reaction give product( Non Polar) with very similar rf how i can separate them 0Fri Nov 10
Which of the following solvent pairs can be used for recrystallization? why or why not? Acetone and ethanol, hexane and water, hexane and diethyl ether 3Sat Nov 11
how to purify long chain alkyldiamine by column chromatography? Which is the best stationary and mobile phase? Which is the best stain fot the compound detection on tlc plate. 0Tue Oct 17
i want to purify my compound by crystallization in ethanol and water, how i can do it 2Mon Oct 23
The 1H experiment is suddenly not sensitive with both ID and SW probe. So I can not get 1H spectrum of my samples (5-20mg). I can only observer solvent peaks and some peaks of samples when increasing nt (128). How I can solve this problem? Thank you for your suggestion. 0Mon Jul 24
how to remove(3-(trifluoromethyl)phenyl(phenyl))methanol from the reaction? 0Fri Jul 21
how to count Rf from two dimension developt? 0Sat Jul 15
how to use the result of TLC where is with two dimension developt on flash column?Can that eluent avaliable for flash column? 0Sat Jul 15
On the TLC eluent, can we mix acitic acid n ammonium hydroxyde in one eluent? 0Thu Jul 13
my sample from latex Antiaris toxicaria, Lesch. what are suitable eluen compose to separate on TLC silika gel. n what good solvent to dissolve the extract for spotting? 1Fri Jul 14
In the TLC , I used n-butanol :aceticacid: water in 4:1:5, but the elution is not uniform, the solvents are eluted separately from the water , what tis the solution of this problem? 0Mon Jul 10
why diastereomers are different compounds,(MP,solubility,Polarity, Nmr) though chemical composition is same , only orientation in space is different ? 1Fri Oct 27
wht happenig when we add naoh during the work up of lah 0Mon Jun 19
HCl in Dioxane 2Fri Jun 16
How can I reveal Ethylene Carbonate using TLC? What solvents or reagents can I use? 0Fri Jun 9
what's the arrow pushing mechanism for the syntheis of dilantin? 0Mon May 8
How to remove Benzyl Alcohol after reaction? 4Mon Jul 17
my nmr contains a peak at 1.47 delta ppm which is not my compound peak and not solvent residual peak what should i do 3Tue Oct 17
Is there an easy way to react a terminal alkyne to a thiol keeping both functional groups 0Tue May 2
how does urea quench sodium nitrite? 0Mon May 1
which runs lower on TLC benzoin or benzil 3Thu Aug 3
how to select column elution 2Wed Aug 16
My compound is highly soluble in water and sparingly soluble in organic solvents liek MC, EA, how can I separate my compound from other similar byproducts? ? Crystallization doesnt seem possible. 2Tue Jul 11
my spots run out with the solvent, did not separate 3Thu Jul 13
HPLC/TFA purification of a primary alochol resulting the formation of TFA-ester, how to remove TFA in AcN/H2O 1Thu Jun 22
in tlc of reaction benzoyl chlorideand hydrazine hydrate benzoylchlorede spot and product spot comes where. i n product and reactant which is more polar. 0Wed Feb 1
my reaction is benzoyl chloride and hydrazinehydrate .i kept in benzene but dimer formed how iget mono. 2Mon Sep 11
What is better method to protect the Boc group and Deprotect the same. 4Thu Sep 7
During workup after the LAH reduction(used for the reduction of P-Cl bond to P-H bond), While workup though the sepeteration of ether and aqeous layer is good, but the ether layer contains some emulsion, which contains water, What I have to do to get a clear organic layer. 3Mon Feb 27
how do purify a solid only soluble in MeOH, EtOH, and H2O? recrystallization seems to be tricky 1Fri Jan 27
how to work up a mitsunobu product of a relatively polar compound 1Fri Oct 27
I have carried a reaction of different piprazines for aryl derivatives but found the sepration of the product so formed because during the column chromatographyboth amine and the product elutes even in first or second fractions. 0Sun Aug 28
I am working on a small scale reaction (1 ml-3 ml) with a very viscous solvent (1000x more viscous than water). Do you any suggestions on how to stir this reaction mixture? 3Sat May 13
What is the best way to minimize solid losses while vacuum filtering? 3Thu Sep 21
i have a mixture of phenols.i find it very hard to get the separation done very well coz all components hav very close Rf vales.what can i do ? 3Wed Sep 7
Can the same plate be used simultaneously for locating different components using different spraying agents? 2Wed Jun 14
Can an excessive amount of cotton wool affect the column resolution? 1Thu Jan 19
I can' revel the N-acetylglucosamin on TLC silice. Is there a specific revelation for this oligossacharide? 1Sat Jun 17
what precautions should be carried out to avoid the blockage of column after chromatography? 1Fri Aug 19
Why does all the silica gel flake off my glass plate as soon as I immerse the end in liquid? (water, 5 mM EDTA, etc) 4Thu Apr 19
I separate two isomers of carotene in a flash chromatography column, using silica gel adsorbent and using ethyl acetate/hexane eluent. When the polarity is reduced, the position of two compound change. In high polar mixture I suppose the trans isomer is that has reduced retention. Is it possible to happens? 1Fri Mar 25 2005
Why doesn't the nitro group show dipole reactivity? 4Thu Nov 23

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